doingdishes
Well-Known Member
http://www.marijuanagrowershq.com/decarboxylating-cannabis-turning-thca-into-thc/
Easy Steps to Decarboxylation
Consumer grade ovens are not always exact so I decided to shoot for a decarboxylation temperature of around 240° Fahrenheit. This should produce quick results without losing any medicinal potency. 30 minutes seemed like a nice round number for a first test and should give the kief and trim plenty of time to come up to temperature.
Kief has a tendency to ball up in the bag which could lead to uneven temperatures and possibly uneven decarboxylation. Before I put it in the oven, I loosened up the clumps with a fork. While most of the trim was already fairly broken up from its time in the kief tumbler, there were still some budlets in the trim that I wanted to break apart.
A few minutes in the Cuisinart works great for breaking up trim and also works well on buds if you have a bunch of joints to roll. The static from the plastic separated out some low grade kief which loosely clung to the lid of the Cuisinart. I brushed this back into the trim.
I placed a pizza stone on the middle rack of the oven and set the oven dial to bake at as close to 240° Fahrenheit as possible. Ovens lose a lot of heat when the door is opened and sometimes the temperature spikes with little explanation. The pizza stone absorbs the heat and helps maintain a constant temperature. In order to track my temperature accurately I used a thermometer with a heat resistant cord. I placed the thermometer on the pizza stone and the digital readout on the counter next to the oven where it could be monitored.
Once the temperature reached about 240° and did not appear to be increasing I placed a small Pyrex bowl of kief and another of the trim on the pizza stone. I set my timer for 30 minutes and continued to monitor the temperature. A Pyrex lasagna dish would be perfect for larger quantities. As expected, the temperature fell a few degrees from opening the door and then came back up to temperature. Throughout the half hour the temperature rose and fell several times for no apparent reason but stayed between 229° and 245° Fahrenheit.
After 30 minutes I removed both Pyrex containers with an oven mit and placed them on the counter to cool. Both the kief and the trim had noticeably fluffed up and gave off a slightly roasted scent. I took a few grams of each and packaged them for lab testing.
I returned the Pyrex dishes to the oven and set the timer for another half hour. I was pretty sure that 30 minutes had been enough to mostly decarboxylate the kief and trim, but just in case I wanted a backup test at a full hour. Either way I had to be patient and wait a few days for the test results to come back.
Results of Decarboxylation Experiment
The following charts show the results of the 30 minute and 60 minute decarboxylation experiments. Also included are the lab results from testing done prior to any artificial decarboxylation to establish a starting point. Note that because of the age of both the kief and the trim, decarboxylation had begun to take place to some degree naturally. This may not be your starting point, but should not affect the results of the experiment much.
Kief
Compound Before Decarb 30 Min Decarb 60 Min Decarb
THCA 24.5% 2.6% .1%
THC 3.8% 25.4% 25.5%
CBDA .6% .3% .3%
CBD 0% 1% .1%
CBN .4% 1% 1.4%
Moisture 0% 0% 0%
Total Cannabanoids 29.3% 30.3% 27.4%
Cannabis Trim
Compound Before Decarb 30 Min Decarb 60 Min Decarb
THCA 6.5% 2.9% .2%
THC .6% 4.8% 6.9%
CBDA .2% .2% .1%
CBD 0% 0% .1%
CBN 0% 0% 0%
Moisture 3.4% 4.5% 0%
Total Cannabanoids 7.3% 7.9% 7.3%
Testing provided by SC Labs
As you can see from the two charts, 30 minutes was not quite enough to completely decarboxylate either the kief or the trim. At 30 minutes the kief was about 90% decarboxylated but the trim was only about 60% decarboxylated. This difference is likely because the trim had a higher starting moisture content. After 60 minutes however, both keif and trim samples were close enough to 100% decarboxylation for my satisfaction.
So there you have it. 240° F for 60 minutes should be enough to decarboxylate any cannabis with a reasonably low moisture content. For material with higher moisture content, the time can be extended but the temperature should not be increased. If you are concerned about losing organic compounds, lower heat can be used but the time should be extended to compensate.
Easy Steps to Decarboxylation
Consumer grade ovens are not always exact so I decided to shoot for a decarboxylation temperature of around 240° Fahrenheit. This should produce quick results without losing any medicinal potency. 30 minutes seemed like a nice round number for a first test and should give the kief and trim plenty of time to come up to temperature.
Kief has a tendency to ball up in the bag which could lead to uneven temperatures and possibly uneven decarboxylation. Before I put it in the oven, I loosened up the clumps with a fork. While most of the trim was already fairly broken up from its time in the kief tumbler, there were still some budlets in the trim that I wanted to break apart.
A few minutes in the Cuisinart works great for breaking up trim and also works well on buds if you have a bunch of joints to roll. The static from the plastic separated out some low grade kief which loosely clung to the lid of the Cuisinart. I brushed this back into the trim.
I placed a pizza stone on the middle rack of the oven and set the oven dial to bake at as close to 240° Fahrenheit as possible. Ovens lose a lot of heat when the door is opened and sometimes the temperature spikes with little explanation. The pizza stone absorbs the heat and helps maintain a constant temperature. In order to track my temperature accurately I used a thermometer with a heat resistant cord. I placed the thermometer on the pizza stone and the digital readout on the counter next to the oven where it could be monitored.
Once the temperature reached about 240° and did not appear to be increasing I placed a small Pyrex bowl of kief and another of the trim on the pizza stone. I set my timer for 30 minutes and continued to monitor the temperature. A Pyrex lasagna dish would be perfect for larger quantities. As expected, the temperature fell a few degrees from opening the door and then came back up to temperature. Throughout the half hour the temperature rose and fell several times for no apparent reason but stayed between 229° and 245° Fahrenheit.
After 30 minutes I removed both Pyrex containers with an oven mit and placed them on the counter to cool. Both the kief and the trim had noticeably fluffed up and gave off a slightly roasted scent. I took a few grams of each and packaged them for lab testing.
I returned the Pyrex dishes to the oven and set the timer for another half hour. I was pretty sure that 30 minutes had been enough to mostly decarboxylate the kief and trim, but just in case I wanted a backup test at a full hour. Either way I had to be patient and wait a few days for the test results to come back.
Results of Decarboxylation Experiment
The following charts show the results of the 30 minute and 60 minute decarboxylation experiments. Also included are the lab results from testing done prior to any artificial decarboxylation to establish a starting point. Note that because of the age of both the kief and the trim, decarboxylation had begun to take place to some degree naturally. This may not be your starting point, but should not affect the results of the experiment much.
Kief
Compound Before Decarb 30 Min Decarb 60 Min Decarb
THCA 24.5% 2.6% .1%
THC 3.8% 25.4% 25.5%
CBDA .6% .3% .3%
CBD 0% 1% .1%
CBN .4% 1% 1.4%
Moisture 0% 0% 0%
Total Cannabanoids 29.3% 30.3% 27.4%
Cannabis Trim
Compound Before Decarb 30 Min Decarb 60 Min Decarb
THCA 6.5% 2.9% .2%
THC .6% 4.8% 6.9%
CBDA .2% .2% .1%
CBD 0% 0% .1%
CBN 0% 0% 0%
Moisture 3.4% 4.5% 0%
Total Cannabanoids 7.3% 7.9% 7.3%
Testing provided by SC Labs
As you can see from the two charts, 30 minutes was not quite enough to completely decarboxylate either the kief or the trim. At 30 minutes the kief was about 90% decarboxylated but the trim was only about 60% decarboxylated. This difference is likely because the trim had a higher starting moisture content. After 60 minutes however, both keif and trim samples were close enough to 100% decarboxylation for my satisfaction.
So there you have it. 240° F for 60 minutes should be enough to decarboxylate any cannabis with a reasonably low moisture content. For material with higher moisture content, the time can be extended but the temperature should not be increased. If you are concerned about losing organic compounds, lower heat can be used but the time should be extended to compensate.
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Notice 30 minutes got most of the kief de-carbed? Over time I've noticed that spreading it thin works well within the 1/2 hour mark. Problem with longer is I've read and seen lab tests that show it will degrade if left too long but if you chop trim and lay the trim/kief out in a thin layer the 30 min works well @250F. Cheers and thanks for the detailed post!
