2lb bho run w/hot water bath purge, help?!

I won't bore anyone with extreme detail I have here pictured a run of some fresh trim mostly popcorn and shake high quality. 2lbs. About 50 cans of 7x butane ran through(too much?) a thin 18 inch tube into a lukewarm Pyrex. It was kept at around 100° as high as 150 at the statt in a hot water bath on a griddle for the past 14 hours and still sparkles and crackels when lit. Does it need a longer purge possibly at a higher temp? I wanted to keep it as close to wax as possible. Easier to handle IMO. Any input is greatly appreciated. Also what's up with the dark color? It turns gold when whipped but looks very brown before hand. The trim was quality so that's not the issue

I realize whipping traps butane. Found that out the hard way in my quest for golden butter. Mine looks like a freshly molded wonka bar

Probably traped moisture in the oil

looks like nutella..then natural peanut butter lol...

james murphy said:

looks like nutella..then natural peanut butter lol...

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Was there any point to this? It was a serious question. If you don't have anything constructive to say please keep your comments to yourself

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hells canyon genetics said:

Probably traped moisture in the oil

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hells canyon genetics, post: 11853101, member: 908463"]Probably traped moisture in the oil[/QUOTE]
Is there a preferred method for removing the water? Its been on a griddle in a 100-120° hot water bath for a full day I feel like its overkill at this point. There is no sizzle or spark when touched with a flame

You need a vacuum oven.

Gorillajdubs said:

You need a vacuum oven.

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I'm getting a whole set up on the 5th but until then do I have any options? Its dark now and pretty clear but still sticky sap. I would much rather have shatter or wax. Something easy to handle

Put a lid on it and don't touch it wait for your vacuum oven, purge for a minimum of 24 hours in the oven.

If you can't wait take a small sample and put it in a hot car on the dash for a day or two. Use parchment paper obviously.

Gorillajdubs said:

Put a lid on it and don't touch it wait for your vacuum oven, purge for a minimum of 24 hours in the oven.

If you can't wait take a small sample and put it in a hot car on the dash for a day or two. Use parchment paper obviously.

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Would a diy hand pump with a brake bleeder do it any justice? I could leave it in the bath at 110°. I've also read about leaving it under a 100w for a few hours. I really do appreciate the input thank you!

What pressure and temps are recommended for the vac oven/chamber? I know boiling points go down at the pressures needed so does that mean I would have to stagger my heat source temp?

Hand pump will work, the oil should be warm to help facilitate the butane removal.

I used a baby food jar many years ago with a hand pump, put a couple grams on a piece of parchment paper begin pumping watch slab expand and then collapse in on itself. Water is the enemy here, keep away from moisture. Pump it until your hand hurts then pump some more. Should hold you over tell you get your oven.

This is it currently. Horrible phone camera my apologies

In the oven you want to run full vacuum, temp and times will be what you experiment with I would not go over 130f and no less the 95f 24-48 hours should be good.

Looks a little dark, lay off the heat. Could also be because its thick hard to say.

get rid of the water bath

Gorpound [QUOTE="Gorillajdubs said:

Looks a little dark, lay off the heat. Could also be because its thick hard to say.

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post: 11856550, member: 908577"]Hand pump will work, the oil should be warm to help facilitate the butane removal.

I used a baby food jar many years ago with a hand pump, put a couple grams on a piece of parchment paper begin pumping watch slab expand and then collapse in on itself. Water is the enemy here, keep away from moisture. Pump it until your hand hurts then pump some more. Should hold you over tell you get your oven.[/QUOTE]
Sick!

Gorillajdubs said:

Looks a little dark, lay off the heat. Could also be because its thick hard to say.

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Ya its two pounds of high quality popcorn and trim in that tiny container but I would not doubt that its burned its extremely thick. Thanks for the quick replies! I will try out the hand pump for now and post a picture when im finished. Next time I will not blast so much at once without a proper set up.

When spread thin it is a beautiful clear amber but is just a tiny bit too sticky. Almost shatter but not quite. Hoping I can turn it around!

You can most definitely turn it around, that vacuum oven is the key though.

Well if your getting the oven then you should be good but still do it in smaller batches in there. And yes watch the temps. There are some great threads in the concentrate section. Some tables you should look at are the boiling point of THC at different pressures/temps. Wouldn't want to boil away any goodness now lol.