Winterizing BHO gone wrong... help

ganjalove90

New Member
Alright rollitup, I don't spend much time on here but I think my current situation requires some insight from the extraction army....

I have about 200 runs under my belt and decided to try some new techniques, aka winterization. Now, I have searched and searched for information more detailed about the process and always come up short. Therefor, this is all pretty new to me and understanding it has almost become my worst nightmare... What seemed to start off well, took a turn for the worse no doubt.

After extracting 1 1/2 lbs of some straight fire, I really need to figure out what's going on over here! :confused::evil: I did my normal process and blasted into pyrex, followed up by dissolving my oil into some everclear.. the reaction was pretty impressive and immediately it began to separate as planned. After I felt it was dissolved, I stuck it in the freezer/dry ice for a little over 24 hrs. The results were immaculate and ready to be poured. After filtering the wax/lipids out of my oil, I was left with a clear yellowish liquid with what seemed to be no plant matter. The pyrex sat out for a few days, no heat, and I was letting it evaporate on its own when I noticed coagulation on the bottom of the pyrex that had trickled its way through filters. Soo0o0o0o, my brain thought it was a good idea to try to refilter what I was left with (as I really wanted to experiment) BUT THIS WAS THE WORST IDEA EVER. NOW, i have what looks like a milkshake sitting in my freezer. It seems like it turned it into a similar residue to whats leftover after you clean your bongs/pipes with ethanol, but I don't quite understand how to fix it, what it means, what I did... etc. If anyone has any answers, pointers, etc....feel free to point me in the right direction. I mean seriously, I has a milkshake in da freezer. I tried to filter a small amount out to see what would happen, straight negative results! :hump:

Any advice would be appreciated. Thanks rollitup ;)
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ganjalove90

New Member
NOOOOOOO,
I really want to knowwww! Will a purge help this?! WTF HAPPENED. Is this even okay for human consumption after it evaporates. WHY IS IT WHITEEEE. Its been in the freezer for like 5 hrs without doing shit. 60lbs of dry ice, no bueno :( Dont be a jerk, help me. :evil:

wow.......
 

JointOperation

Well-Known Member
the only thing i can suggest . is to just add some sort of heat . .and start your purge and see what happens.. just make sure u stir this up so that watever left over shit u missed during the filtering.. is spread.. i had this happen.. and it ended up coming out halfway decent.. but u want to get a buchner funnel and use a pump to filter.. this will get as much as u can get out of it .. and also.. wait the 36-48 hours with the dry ice or freezer. .. and then filter.. it sounds like u were rushing a lil. see if adding heat gets u to a clear state.. if not. i really hope u didnt do your entire thing of oil in 1 shot as a first time winterize.. because u should always do a small amount and get it right.. then do more.. never put all your eggs into 1 basket..

but if anything i say.. add fucking heat.. get your temps up to atleast 105-150 .. try to purge.. i mean.. shit .. if u had a good product to begin.. then u got alot of wax and shit out.. and now u purge.. u have a product that has less wax then it started.. it should be fine.. just not a full winterization.. u mixed it up.. is all. u need to get the temps down to 0F.. so if i was u .. check to see what temp u are getting it to.. if its not 0F then maybe u can get it lowered and have the shit seperate again.. if not i dont see any issue with just purging it .. see wat happens.
 

hyroot

Well-Known Member
The cleanest bho in general is not safe for human consumption. All the chems are still there in the end. The worst of all is cadmium and benzene. Highly toxic and highly carcinogenic. Worst than the propane propellants and acetates. Even lab grade (n) butane has all those chems. Thats why so many people are hospitalized. Not the high THC %
 

qwizoking

Well-Known Member
Maybe try the concentrate and extract section first of all...
second your post doesn't make sense
 

Sirdabsalot462

Well-Known Member
Sounds like your saturation levels are too high....

More Ethanol...
190 right?

Anything else has too much water, which would explain the white.
 

qwizoking

Well-Known Member
After filtering the wax/lipids out of my oil, I was left with a clear yellowish liquid with what seemed to be no plant matter. The pyrex sat out for a few days, no heat, and I was letting it evaporate on its own when I noticed coagulation on the bottom of the pyrex that had trickled its way through filters.

if you already filtered the waxes how did it get back in? coagulation on the bottom after days of evap just sounds like hash precipitating

second, how did you refilter, adding etoh again? You just left most of the important details..would cause the white azeotrope style milkshake, still not expected
 
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