Super Critical Fluid Extraction (S.F.E.)

pharmacoping

Active Member
at that point you'll have what i do, less the expense !.
c02--in my experience it will not extract the way you want it to until you spend money to contain super pressures and temperature automation. the smallest machines I've seen cost a little over 10grand, so I figure 5g to build it, and blow up a few times to get it right. it yields less than butane, which is also food grade fda approved for pharmaceutical extractions of plant oils and compounds.

I've messed with c02 canisters, even the huge ones, and couldnt make this work. I hope you have better luck than me.
 

oilmkr420

Active Member
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Over the years I've had the opertunity to teach several people how to make "honey oil" useing the Supercritical Fluid Extraction method (S.F.E) for short. Many of these people have gone on to reaserch methods of constructing shoestring devices to do the job.


One thing that has always been a concern of mine, is the p.v.c. people use for the main body of these contraptions.
I always felt that this was not the best material for this application.
With this In mind, I went to the internet looking for equipment manafactured to perform this task
I did find one for extracting essetial oils for the holistic healing world.
It had a price tag of $1200! ouch.

The next step was to make a prototype and so I did!
After showing it around a little in the colorado medicinal comunity, I started building them! the parts are fairly expensive to have made up. Cost $380.00 per piece out the door about what a good bubble bag kit costs.

With this device I run all my sugar leaves, fine trim, node scrapings, and underdeveloped undertrash,
I can recover about 7 grams of oil from about 3/4 ounce of garbage. The oil is golden amber in color and drips off a dip stick like honey. So do yourself a favor and treat yourself every crop. Feel free to check out photo album for more pics of extractor and melungeon magic.


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heres my 6,000 and 10,000 psi vessels. the 10,000 vessel was property of nasa, before finding its way to an appropriate home. i like the tight construction you use, maintaining pressure rather easily, what feeds it supply? how much does it hold? tight extractor.
 

oilmkr420

Active Member
i dont think you had proper co-solvent ratios which is an important part of its ability for large recovery. not smaller than butane, but many folds more w out funky tastes.
at that point you'll have what i do, less the expense !.
c02--in my experience it will not extract the way you want it to until you spend money to contain super pressures and temperature automation. the smallest machines I've seen cost a little over 10grand, so I figure 5g to build it, and blow up a few times to get it right. it yields less than butane, which is also food grade fda approved for pharmaceutical extractions of plant oils and compounds.

I've messed with c02 canisters, even the huge ones, and couldnt make this work. I hope you have better luck than me.
 

oilmkr420

Active Member
That's why a pro system costs so much, no one likes shrapnel. I would be content with a reclaim system for now...
306f @ 580psi is simple pressure to contain, that high temp is needed for scfe w butane. most steel vessels weaken beyond 350F. but 38 bar is cake.
 

oilmkr420

Active Member
Working fluid? Temps? Pressures? How manage the super/subcritical transition? I see no hardware for that ... cn
butane is supercritical @ 306F and 580psi. Anything near the critical point is a subcritical extraction. Below that is merely a pressurized extraction @ whatever pressure you extract @.
 

oilmkr420

Active Member
my extraction takes a minute, but the recovery of 100% of the butane takes two hours. it doesnt need to be baby sat at all. and when done the butane back in the sealed vessel waiting another run, saving $$ each times. not sure how much in a vector, but I use/reuse 400grams of liquid butane per run. I extract with 200grams, wait a bit, run the other 200g. couple cans' savings anyway, every time. I had large tane tank for over a year, just got it filled. if in a hurry, this can be evaporated old style outside also,conveniently with an included mile long little hose that seculey attaches.......and out a window. using up the tane though.
There's no way to recover 100% of the butane. A lot gets retained in the tane, making it smaller than 100%. There is a theoretical recovery and an actual recovery. 80% is super high.
 

Markco

New Member
hi, my names is marcos, do you have a plans for build my own Supercritical Fluid Extraction I am student in Mexico City, tanks
 
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